Crystal and molecular structure of bis(8-phenylmenthyl) 2-(2-methyl-5-oxo-3-cyclohexen-1-yl)propandioate, C₄₂H₅₄O₅• CH₃CN

Authors

Dennis W. Bennett, University of Wisconsin-Milwaukee
Tasneem A. Siddiquee, University of Wisconsin-MilwaukeeFollow
Daniel T. Haworth, Marquette UniversityFollow
Subhabrata Chaudhury, Marquette University
William Donaldson, Marquette UniversityFollow

Document Type

Article

Publication Date

8-2-2006

Publisher

Springer

Source Publication

Journal of Chemical Crystallography

Source ISSN

1074-1542

Original Item ID

DOI: 10.1007/s10870-006-9136-y

Abstract

The X-ray crystal structure of the title compound, as crystallized from acetonitrile-water was determined. The relative stereochemistry of the cyclohexenone ring with respect to the 8-phenylmenthyl esters was determined. The title compound crystallizes in the noncentrosymmetric space group P2₁, with a=8.9850(10) Å, b=15.575(3) Å, c=14.478(2) Å, β=94.61(2)°, and D _calc=1.118 g cm⁻³ for Z=2.

Comments

Published version. Journal of Chemical Crystallography, Volume 36, No. 11 (August 2006):777-780. DOI. © 2006 Springer. Used with permission.

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Recommended Citation

Bennett, Dennis W.; Siddiquee, Tasneem A.; Haworth, Daniel T.; Chaudhury, Subhabrata; and Donaldson, William, "Crystal and molecular structure of bis(8-phenylmenthyl) 2-(2-methyl-5-oxo-3-cyclohexen-1-yl)propandioate, C₄₂H₅₄O₅• CH₃CN" (2006). Chemistry Faculty Research and Publications. 33.
https://epublications.marquette.edu/chem_fac/33