Crystal and molecular structure of a steroidal spirocyclic lactone, C29H32O4

Authors

Dennis W. Bennett, University of Wisconsin - MilwaukeeFollow
Tasneem Siddiquee, University of Wisconsin - MilwaukeeFollow
Kristen L. Murphy
Daniel T. Haworth, Marquette UniversityFollow
Zhengjie HeFollow
William Donaldson, Marquette UniversityFollow

Document Type

Article

Publication Date

2003

Source Publication

Journal of Chemical Crystallography

Abstract

The X-ray crystal structure of the title compound, as crystallized from methanol–methylene chloride was determined. The asymmetric unit contains two steroid molecules, which differ primarily in the orientation of the aromatic rings of the benzyl ethers. The title compound crystallizes in the noncentrosymmetric space group P2(1), with a = 7.558(2), b = 16.673(3), c = 18.735(4) Å, ß = 97.610(10)°, and D _calc = 1.268 g cm^–1 for Z = 4.

Comments

Journal of Chemical Crystallography, Vol. 33, No. 11 (2003). pp 897-902. DOI: 10.1023/A:1027418131808

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Recommended Citation

Bennett, Dennis W.; Siddiquee, Tasneem; Murphy, Kristen L.; Haworth, Daniel T.; He, Zhengjie; and Donaldson, William, "Crystal and molecular structure of a steroidal spirocyclic lactone, C29H32O4" (2003). Chemistry Faculty Research and Publications. 62.
https://epublications.marquette.edu/chem_fac/62