Crystal and molecular structure of a steroidal spirocyclic lactone, C29H32O4
Journal of Chemical Crystallography
The X-ray crystal structure of the title compound, as crystallized from methanol–methylene chloride was determined. The asymmetric unit contains two steroid molecules, which differ primarily in the orientation of the aromatic rings of the benzyl ethers. The title compound crystallizes in the noncentrosymmetric space group P2(1), with a = 7.558(2), b = 16.673(3), c = 18.735(4) Å, ß = 97.610(10)°, and D calc = 1.268 g cm–1 for Z = 4.
Bennett, Dennis W.; Siddiquee, Tasneem; Murphy, Kristen L.; Haworth, Daniel T.; He, Zhengjie; and Donaldson, William, "Crystal and molecular structure of a steroidal spirocyclic lactone, C29H32O4" (2003). Chemistry Faculty Research and Publications. 62.
Journal of Chemical Crystallography, Vol. 33, No. 11 (2003). pp 897-902. DOI: 10.1023/A:1027418131808
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