Date of Award

Spring 1979

Document Type

Thesis - Restricted

Degree Name

Master of Science (MS)

Department

Mechanical Engineering

First Advisor

Blumenthal, Robert N.

Second Advisor

Seitz, Martin A.

Third Advisor

Hirthe, Walter M.

Abstract

A nonequilibrium dynamic technique was used to measure the electrical conductivity of .1 and .5 mole % Ta205 doped Ceria (Ce1-yTay02-x with y = .002 and .010 respectively) as a function of temperature between 1000 and 700°C near stoichiometry (in oxygen) and at several nonstoichiometric compositions between x = . 001 and .1. The conductivity at each composition was characterized in the form "formula" Although the results were reasonably consistant [sic] with equilibrium conductivity data previously obtained at 1000 and 800°c2, the activation energy (Q) exhibited a nonlinear dependence on x which was in contrast with previous representations of the conductivity of nonstoichiometric Tantalum doped Ceria. The results appear to discount an interpretation of the conductivity in terms of a simple defect structure and indicate a complex roll of the dopant defects !n the conduction mechanism. Similar measurements were also carried out on pure nonstoichiometric Ceria over an equilvalent [sic] temperature and compositional range. The activation energy in this case was consistent with a linear dependence on x.

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