Date of Award

Summer 1989

Document Type

Thesis - Restricted

Degree Name

Master of Science (MS)

Department

Foreign Languages and Literatures

First Advisor

Fournelle, Raymond A.

Second Advisor

Hirthe, Walter

Third Advisor

Brantley, William A.

Abstract

The superelastic behavior of cold drawn and annealed Ti-50.8at.%Ni alloy wire has been investigated by tensile testing, differential scanning calorimetry (DSC) and light microscopy. Annealing of the wire at 400°C has been formed to induce superelastic behavior in it. Annealing at higher temperatures ( 450-600° C) was formed to result in no superelasticity, while annealing at still higher temperatures (650- 750°C) resulted in partial superelasticity. The changes in superelastic behavior with annealing has been associated with the reversion of some or all of the cold worked martensite and R phase in the cold drawn wires to austenite, and with the variation of the austenite finish Af temperature of the reverted austenite with annealing temperature. This variation of Af is related in a complicated way with the residual stresses left in the reverted austenite as well as precipitation of nickel rich compounds (Ti11 Ni14 and Ti2 Ni3) in it. The superelastic behavior, microstructure, and transformation behavior of commercial superelastic orthodontic wires (Sentinol [sic], Ormco and Korean) have also been investigated for comparison. These wires were all found to have superelastic behavior, microstructures, and transformation behavior similar to the Ti-50.8at.%Ni alloy after annealing at 400°C.

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