Synthesis and X-ray structural Investigation of 6-Chloro-10-Phenyl-1,2,3,4-Tetrahydroacridine

Authors

Igor I. Ponomarev, Institute of Organometallic CompoundsFollow
O. V. Shishkin, Russian Academy of SciencesFollow
Sergey Lindeman, Marquette UniversityFollow
Yu. A. Volkova, Russian Academy of Sciences

Document Type

Article

Language

eng

Publication Date

8-1994

Publisher

Springer

Source Publication

Russian Chemical Bulletin

Source ISSN

1066-5285

Abstract

An X-ray structural study of 6-chloro-10-phenyl-1,2,3,4-tetrahydroacridine prepared by the reaction of cyclohexanone with 2-amino-5-chlorobenzofenone was carried out. At 20°Ca=24.215(6),b=8.967(2),c=15.006(3) Å, β=115.57(2)°,V= 2939(1) ų,d_calc=1.310 g cm⁻³,Z=4, space groupC2/c, 1324 reflections, λMoKα,R=0.038. The cyclohexene ring has a half-chair conformation. The phenyl substituent is rotated 71.2° with respect to the plane of the quinoline fragment.

Comments

Russian Chemical Bulletin, Vol. 43, No. 8 (August 1994): 1390-1391. DOI.

Sergey Lindeman was affiliated with Russian Academy of Sciences at the time of publication.

Recommended Citation

Ponomarev, Igor I.; Shishkin, O. V.; Lindeman, Sergey; and Volkova, Yu. A., "Synthesis and X-ray structural Investigation of 6-Chloro-10-Phenyl-1,2,3,4-Tetrahydroacridine" (1994). Chemistry Faculty Research and Publications. 669.
https://epublications.marquette.edu/chem_fac/669